Oily yellow dmt. naptha taken out and placed into jar and put into freezer.

Oily yellow dmt 4. 5ph) formula added and left for 2 hours. e. 5 grams (yes, 1500mg) of mainly off-white dmt soft crystals, with small amounts of yellow conglomerations. The orange color must come from something else, since a yellow oxidation product couldn't turn a translucent crystal orange. . One person may have yellow dmt that is 95% pure while another may have 50%. Feb 26, 2008 · One home extractor who did some TLC analysis on whole and purified extracts of Mimosa root bark described DMT N-oxide as a yellow oil, though I can't corroborate this decription in the published literature. Indeed n-oxide is not soluble in naphtha/heptane (unless of course your naphtha has traces of aromatics like xylene, which does happen often enough and is responsible for some people using naphtha and getting a red/orange product). 5 hours. the property that allowed me to separate the two was that the yellow stuff would typically bind to the glass, and i could scrape the majority of the dmt crystals off, leaving the yellow stuff behind. Does the oils left in the naptha effect the solubility of dmt or can I continue using this oily naptha as long as I strip the dmt from it? A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along with routes of administration (ROA), as well as a central repository for extraction guides and ingestion methods. White was fractol imagery and yellow always was a spiritual hyperspace breakthrough. First I tought the layers didnt seperate but after looking at it through daylight I saw the difference, so I pulled it out and put it in my glass dish like I always do, and put it in the freezer, I just took it out after a couple of hours to check it out but there is a very dark brown oily good on the bottom and above that there are dark yellow Feb 16, 2024 · I believe that 5-meo-DMT-N-Oxide has a pale brown color, which can appear orange in concentration and yellow in dilution. I've heard that DMT that is yellow/orange has a compound called yureamine that contributes to a darker/dirtier spice experience from darker DMT. Biased on any personal level. It's not goo. naptha taken out and placed into jar and put into freezer. Both/all of the above. We are not speaking of color, as it is fairly well known that yellow DMT can be just as pure as white DMT… however, there are things you can do to improve the overall quality of your product, which will make growing these large rocks a lot easier (defat, water wash, carbon wash etc. 75g Calcium hydroxide mixed in and stirred thoroughly. Remember to flair your posts and choose an appropriate user flair. Sep 15, 2022 · I've been thinking for a while this is sort of a "total extract' which gets both the spice and miscellaenous plant lipids, mostly because the freeze precipitation tends to yield both white fluffly crystals and an oily yellow substance, but I recently did a bioassay of the yellow oil and it was certainly very active, which leads me to believe What is the yellow oil/goo that makes into the the extract? I thought that it was plant fats left behind during A/B extraction but I still get some even after defatting during A/B extractions. · High quality NPS – you should be able to use naphtha, but if you can get your hands on heptane, hexane, bestine etc. crystalization was sped up by scratching the surface of the 'oil' with a needle. crystal polymorphism - DMT has a property that allows it appear yellow or white, regardless of make up NMT - yellow could be a result of NMT bring in the final product oxidation - everything oxidizes over time. To make the oil turn into crystal you dissolve it with an excess of solvent and the freeze precipitate again, or you can just scrape it and it will likely just crystalize within 24hrs. The DMT will already be melting if the water is hot enough. I think someone said fats can make it yellow White - generally pretty clean product Purple - people claim Im pretty sure I have the N-oxide because that is exactly what happened I left a blowdryer blowing hot air right into the solvent making it swirl around. DMT’s psychological effects are mostly due to its binding to the 5-HT2A receptor, which is found mostly in areas of the brain associated with high-level cognition: self-awareness, emotions and introspection. One is just curious as to if the yellowing is just plant fats and other tryptamines (since it probably came from reused naphtha that wasn't washed and there's no telling how long it may have been crystallizing in a freezer) or if it may be something one should be concerned about. NO SOURCING ANYTHING related to this… Consistency: 60-70% light yellow powder soft to the touch, 30-40% dark yellow gel like chucks of oily material. You can convert all your DMT to DMT N-Oxide by heating the DMT to it’s melting point and blowing a fan over it. 4 Delafonze19's Preparation of Yellow Spice Oil). May 30, 2008 · There is a small impurity (abundance ~2) at 205. D-limo is still very much yellow-orange (looks like it toned down a little through the salting process). Add the hot solvent little by little (eye-dropper), agitating until all of the DMT is dissolved. However a slight impurity (1% or less) can give the yellow color. I it is that yellow impurity causing the colorationg, it will stay dissolved int the NPS and the N,N-DMT will precipitate back out. To start: Followed Jorkest's tek to the T. Naptha was pour out and Crystals were collected. is this stuff the real deal or is it possible its been washed or something prventing an extraction. May 30, 2008 · We've already fingered a yellow oil as the most likely candidate for the simplest DMT oxidation product (DMT N-oxide). I'm just stating you want the yellow stuff with the alkaloids. The problem with DMT N-Oxide is that it is an oil that won’t crystallize. Cooking setup: Residue felt to dry: Total yield 2. Similarly to how it travels from the basic solution to the NPS above in an A/B or STB extraction. First remove the ether from your solution (evap for example in a well ventilated area or outside?) then add the hexane to pull the DMT without the oils. Color does not matter, despite what some will tell you, yellow DMT can be just as pure as white DMT… however, we need to ensure there is no oily residue or traces of plant fats AT ALL, as it will affect crystal type. We’re a community connected by N,N-Dimethyltryptamine. If you dissolve everything into a minimal amount of hot/boiling NPS (<100C). Does the oils left in the naptha effect the solubility of dmt or can I continue using this oily naptha as long as I strip the dmt from it? Nov 23, 2016 · But it can also be other things:-Oily non-volatile impure solvent remains (bad to smoke)-Plant oils/fatty acids or other natural impurities (more likely ok to smoke, and can even make for a more efficient vaporization as it protects spice from the lighter's heat, though might taste a bit harsher)-DMT N-oxide mixed in any proportions to DMT (ok Its a pain to get rid of because it precipitates from the heptane i was using at about the same rate as the dmt. My logic was always the white stuff is probably more pure than the colored. We've already fingered a yellow oil as the most likely candidate for the simplest DMT oxidation product (DMT N-oxide). I think something like 1 hour is all that’s needed. Posted by u/Cohan1090 - 2 votes and 2 comments SWIM is pretty sure this is either DMT-n-oxide or "jungle DMT" (SWIM's tests suggest jungle DMT is very slightly soluble in naptha) because it is soluble in vinegar and though he hasn't bio-essayed it alone, when the crystals and goo are smoked together they seem just as potent per mg as smoking only the crystals. Dmt is a extremely powerful compound so it really doesn't matter. The yellow crystals or powder that are a result of freeze precipitation and the yellow crystals and goo that is a result of evaping the left over naphtha after an stb freeze precip, its all good stuff the key to enjoying this stuff is proper ingestion. after doing that about 3 times, i Jun 30, 2024 · -0,5g yellow/darkish yellow crystals dissolved in warmed up 20ml solvent (brake cleaner, temperature just a shot in the dark, hot water bath with no thermometer, I dont have one atm that goes above 50°C). Posted by u/Outrageous_Holiday_4 - 17 votes and 25 comments Tried clay as well and saw no problems. The solvent will be a clear yellow. If the yellow precipitates back out, then it's just the N,N-DMT. 12 On a related note, one home extractor has discovered a method for reliably converting bright white spice into a yellow oil (without "Polymorphs and DMT with an oxidized pyrrole ring appear yellow to red — even viscous and oily! — and is 100% DMT. Has anyone else I have some Acacia DMT tincher in 190 proof grain alcohol and is quite active But ive had the more pure crystals before and prefere their effects over the waxy DMT oil in photos below. What you have heard about the yellow stuff being DMT is true however it is more NMT which has a different boiling and freezing point than DMT. For a casual DMT smoker, there is absolutely nothing wrong or inferior with DMT that is yellow crystal, white crystal, orange goo, white goo. At room temperature it forms slowly over the course of a few years. After that Swim did a freezer precipitate. if u let it settle Aug 16, 2012 · ß resulted in almost 1. But it can also be other things in some cases :-Oily non-volatile impure solvent remains, if you use a solvent that doesn't evaporate clean (bad to smoke) Apr 21, 2017 · The yellow can be a number of things. Had some stored for over two weeks and didn't notice any changes in effects. Also, this forum really discourages the whole "SWIM" thing. I've read a bunch of reviews with same experiences as mine. My question is about the re-use of that naptha. I usually use a STB tek, and the more pulls I do the yellower the crystals get. Downside to adding more lye is the dmt could be more oily/ yellow due to more impurities due to higher pH. How about DMT that is still damp and a deep orange hue? What alkaloids would be expected to be presant? Am i correct to asume that i must first compleatly evaporate the alcohol tincher . Third, dmt is polymorphic, and if you used heat during the extraction process it tends to be more yellow and also precipitate out as oil. I have some Acacia DMT tincher in 190 proof grain alcohol and is quite active But ive had the more pure crystals before and prefere their effects over the waxy DMT oil in photos below. I'm fairly confident that I couldn't tell a difference between any of the samples in a blind test. The small dropper bottel contains grain alcohol with dmt oils. Conversely, white product does not necessarily indicate pure DMT, only means it Contains only substances which are white, which includes virtually all alkaloids. 12 On a related note, one home extractor has discovered a method for reliably converting bright white spice into a yellow oil (without Yellow DMT isn’t really what people call jungle spice. Maybe not green goo, though There most likely won't be a noticeable difference between white or yellow product. You can get it by doing very hot pu so xlogp says noxide is insol in naphtha and heptane yet i get beautiful orange to yellow spice using both naphtha and heptane. "Polymorphs and DMT with an oxidized pyrrole ring appear yellow to red — even viscous and oily! — and is 100% DMT. using q21 tek 2 fluffy white fun fest, only diffence from now and previous great results is product and it was Feb 14, 2025 · This site uses cookies to help personalise content, tailor your experience and to keep you logged in if you register. This is done by adding an acidic solution which stays separated under the NPS layer. then try for freeze percipitation or another atempt at total evaporation to get a cleaner more crystaline spice? Apr 6, 2015 · YOU WILL NOTICE THAT THE DISSOLVED SPICE WILL SEPARATE AND A YELLOW OILY SUBSTANCE WILL SETTLE ON THE BOTTOM, MAINTAINING THE HEAT OF THE HEPTANE WILL HELP THIS SEPARATION OF THE 5-METHOXY-DMT AND THE FREEBASE DMT CONSIDERABLY*** 3. It was just an oilgomer form of DMT. What is the yellow oil/goo that makes into the the extract? I thought that it was plant fats left behind during A/B extraction but I still get some even after defatting during A/B extractions. 100g bark is powdered and has acetic acid (2. when the spice is dissolved in boiling heptane there is an orange layer at the bottom of the beaker, and boiling yellow heptane above that. I have never noticed any difference in effect between white, clear, yellow, orange, red, oily, or waxy DMT extracted from multiple different plant sources. Welcome to /r/DMT. Jungle spice is generally waxy darker orange or red rather than yellow and pulled with xylene after exhausting the bark with naphtha. Pipette off the heptane that is clean into a clean glass dish leaving behind the yellow oily 5-MeO. – not oily, fatty)- so I recommend taking the time to purify your product before moving on. 30mg of yellow = 20 mg of white, so even losing some to a reX isn't that big a deal because you just dose a little smaller. Feb 8, 2011 · Dmt n oxide is a well known mammalian metabolite of dmt but doesn't appear to be present in plant material. Result: about 1. NO SOURCING ANYTHING related to this… The starting material that successfully yielded my first batch of rocks was bone dry (i. 1 m/z, which is most likely accounted for by DMT N-oxide. If you scrape it all up and leave it for a week or more the oily yellow substance will form a smokable wax (if you used naphtha). Anyway, the spice in question is yellow, oily, crystal. Whatever alkaloids come along, great, but the oily bark garbage isn't my cup of tea. in the ordinary world of phytochemical extraction, a simple A/B or STB as done by most nexians, would be said to result in the CRUDE ALKALOIDS. Does the oils left in the naptha effect the solubility of dmt or can I continue using this oily naptha as long as I strip the dmt from it? The tek I use results me with dmt-free yellow oily naptha. in the 90s when the DMT extraction world was a little fresher, and more guided by experienced chemists, there was no obsession with the end-product being crystals. With these plants there is an impurity (presumably lipids) that is yellow. In the hot water bath the impurities will sink to the bottom and you can use a turkey baster to suck up the naphtha (except the impurities at the bottom in the container) and put it on a glass pan to either evaporate or cover with plastic wrap and put it in The tek I use results me with dmt-free yellow oily naptha. . Mar 17, 2024 · For that you can best use Hexane. Extraction 2: STB 40 grams MHRB 20 grams lye 200 ml water 25 ml naptha added lye to water and let stand one hour. Procedure is q21s tek. Hi, simple question I haven't been able to find the answer to after a quick look around I did an STB extraction on 220 gms of mimosa rootbark powder and got ~500 mg mixed whitish dmt and yellow, oily DMT-N-Oxide. My experience with the yellow spice has been very good. It seems like some weight is always lost when recrystallizing something and that when working with smaller amounts of things that the fraction which is lost is From buying and using DMT i've come across a few different colors. Can I just throw 50 mg in some lemon juice and drink it with a maoi? or will only the non-oxidized dmt dissolve and affect my body The tek I use results me with dmt-free yellow oily naptha. I'm guessing with the use of Acuminata and the oily dmt indicates you're from Australia and you used shellite. Jan 1, 2023 · Oiliness can be down to one or more of several reasons and is not necessarily bad. then re desolve the yellow waxy dmt in warm napatha then do . 200ml naphta added and let sit for 4. It seems as though my 3rd/4th/5th pulls are yielding yellow crystals (which look a lot better than this), but on my next extraction I think I will increase the amount of lye to at least 70-80g’s. Always had this problem, and never worked it out. crystalization requires either re-crystalization (up to several times) and/or DMT needs to be in contact with oxygen to form DMT N-Oxide. The yellow was always better no matter what. 332K subscribers in the DMT community. After salting, ended up with highly yellowed fumaric acid solution. • *CLEAN* DMT – I must stress that it is quite important to ensure the starting product is as pure and clean as possible. It comes down to how smooth and pretty you want it to be. As far as I can tell from what happens when we smoke it, the yellow must Pure DMT freebase is a clear oil. me Psychedelic news, articles, interviews and art from the DMT-Nexus and other sources. Hey guys, I'm doing a mini A/B on some yellow naptha pulls from an A/B extraction using this method - Simple clean-up for NPS pulled from ACRB ( mini AB ) - A/B - Welcome to the DMT-Nexus I'm finding that some of the yellow is still making it's way across to the end product. later assay suggested mainly dmt, though it did not completely solidify, reverting to 'putty', often caused by nmt with betacarbolines What freeze precipiatated was almost all DMT. But it can also be other things in some cases :-Oily non-volatile impure solvent remains, if you use a solvent that doesn't evaporate clean (bad to smoke) Dec 8, 2012 · A backsalting can be performed to retrieve the DMT from the cooking oil. Feb 7, 2009 · DMT needs to be in contact with oxygen to form DMT N-Oxide. then opt for this. Body temp is definitely high enough to melt DMT, and even pure white crystaline dmt freebase will turn a little yellow when it melts. One way is to redissolve the oily material in the minimum sufficient warm naphtha (no naked flames!) and then cool it off slowly. The tek I use results me with dmt-free yellow oily naptha. product white DMT while STB extractions produce yellow dmt pretty consistently (although I find that in cold weather the DMT does come out white, Either can yield white/colorless, yellow, or a number of other colors. Oily DMT from evaporated naphtha really ought to be purified, however. 30 mins pass by before naptha is added. It looks great until it's time to scrape. There's more at play than just what is and isn't soluble. Yellow - this stuff is crude in my opinion. Both of these are fine. [carbonate wash several times] . It forms faster as the temperature rises. Use as little solvent as possible. NOW that MHRB is harder to find SWIM got the polvo mentioned above id post a pic but jpeg wont upload. White dmt was never the real deal for me. Posted by u/Least-Yak-3697 - 1 vote and 30 comments Apr 18, 2023 · Emulsion can still be fixed with a by adding a bit more lye (this is more of an issue with ARB bot MHRB). ) 339K subscribers in the DMT community. DMT dissolved in the NPS will travel to the acidic solution below. This is perfectly fine and smokeable. I've noticed a higher concentration of this stuff when the Then you can siphon and leave the other stuff behind. So your yellow dmt isn't going to be the same as someone else's. yellow is most likely plant oils or other plant impurities. It should take only about 20-30ml of solvent per gram of powder. Some copper colored oil was not absorbed, and was left behind on next step. Aug 16, 2008 · So before freezing the solvent, pour it into another container leaving behind all the yellow DMT N-Oxide oil. However, an easy way to make use of the left over yellow DMT N-Oxide oil is to add calcium carbonate to it at a 10:1 ratio of calcium carbonate to DMT N-Oxide by weight. That will not pull the oils, and only grab the non-oily DMT-freebase. Ya, doing an A/B would definitely help. This seems most likely as the intensity of the yield has been verified Which leads me to another concern. By continuing to use this site, you are consenting to our use of cookies. I then evaporated the NPS and a SWIM is actually using calcium hydroxide and has gotten great results in the past. This way you can freeze precipitate the DMT to get pure DMT, and still use the yellow oily DMT N-Oxide which is also hallucinogenic. The extraction is very clean and you can see from the pic the spice came out light yellow when scraped out and mixed. While SWIM has not extracted with lye for a while, pretty sure that just adding a splash of vinegar and some hot water to the MHRB and letting it soak for an hour or more before adding the lye would make the extraction take much shorter cause having the hot-acidic water dissolve the DMT away from the bark and into the water tends makes the PH needed much Feb 25, 2021 · Hi Folks I recently did an extraction on 100g MHRB using this TEK I got 1. then added naptha and agitated for 3 days. Aug 16, 2008 · The problem with DMT N-Oxide is that it is an oil that won’t crystallize. Does the oils left in the naptha effect the solubility of dmt or can I continue using this oily naptha as long as I strip the dmt from it? Apr 14, 2010 · Yellow colour can be a number of things: - Most of the times, yellow DMT is just DMT. If one crystalizes several times from hexane a pure product that if melted is clear can be obtained. Is there a difference in terms of trips? Maybe, some people report white to be more chaotic, while yellow more mellow. Evaporated to a brown goop. Acids can change things about N,N-DMT molecule. Just my sense on it. Ended up with highly orange d-limo (first oddity). This is why you will see some yellow goo with your white crystals when you do your freeze precipitation. I think oxidation is a likely explanation for what is happening. 3g from 100g mhrb: 1g separated into fine and coarse particles: Close up: I read the is your dmt ok to smoke post and wish to do a clean up because: - Final product has dark oily chucks. 5 grams of barley active oily yellow DMT. I have tried a couple different ways to try and make my DMT crystals whiter and purer, but so far the results have not been impressive. Voidmatrix #2. This helps to substantiate the idea that the yellow oil is DMT N-oxide, since the product was collected by evaporation, and was described as "a yellow waxy-crystalline" material. Does the oils left in the naptha effect the solubility of dmt or can I continue using this oily naptha as long as I strip the dmt from it? I've UTSE already. It could be plant fats, NMT, oxidation. Are there any papers that have Id'd dmt n oxide in any plant? The only sort of evidence we have that dmt n oxide might exist is that people have reduced with zinc dust 'yellow' dmt and claimed to have obtained crystals after this. now have a pic of it. Why after evaporation is my DMT very oily? The-Nexian. Electron loss is another form of oxidation, so "oxidised DMT" doesn't necessarily equate to the N-oxide. 7g of mostly white but also a few yellow crystals after freeze precip. Buy some vm and p naphtha from lows, put your deems in a small container that can be put in a hot water bath and fill it with the naphtha. Jun 30, 2024 · It has been more or less established that the coloured, oily, active material consists of oligomers/polymers of DMT formed by electron transfer between the pyrrole rings of DMT molecules. Based on this information, it sounds like these methods are producing DMT which contains the type of yellow oil I suspect to be DMT N-oxide. Pure DMT itself has been shown to be polymorphic , so yellow does not necessarily mean impurities. So before freezing the solvent, pour it into another container leaving behind all the yellow DMT N-Oxide oil. Posted by u/createman1 - 1 vote and 11 comments To start: Followed Jorkest's tek to the T. Evaporated to a brown goop DMT is a molecule that mimics the neurotransmitter serotonin, much like the other classic psychedelics LSD and psilocybin. Apr 14, 2010 · Yellow colour can be a number of things: - Most of the times, yellow DMT is just DMT. It's hard for me to tell if the method storing it actually makes a big difference other than by it reacting with materials, but even then if it has happened to any I had stored I couldn't tell since dmt trips I have always end up being one of around half a dozen "themed" trips So before freezing the solvent, pour it into another container leaving behind all the yellow DMT N-Oxide oil. Delafonze19 has reported happening on a method for reliably converting white DMT to the potent yellow oil (see 32 III. This evaporated 450ml naphtha completely in about an hour and I was left with the yellow goo. It slowly crystallized but was still very oily. lkasil gnptvx vzeazw pyxo xmiqot hsngtt xcllh rnqeu fvgdr xkfgmyr gtgwox diaflh xovdx cwln lbuwnnm